© 2019 Beamex Oy Ab. The purpose of the weighing test is to test the accuracy (calibrate) of the weighing instrument throughout its whole range in several steps, with increasing and decreasing weight. Below picture is a general illustration of unlinearity. There are dedicated regulations for weighing instruments and their calibration (EURAMET Calibration Guide, NIST Handbook 44, OIML); more on those later in the article.In this article, the main focus is to look at the practical considerations and the different tests you should perform when calibrating your weighing instruments. 10 0 obj <>stream 7 0 obj<> 5.6.2 Note the weight. When instrument is calibrated, the results are different with increasing and decreasing calibration points: Minimum weight test is a test that is not always required to be done. For the calculation of the drift 10 mg weight shall be … The above picture is for rectangular and round load receptors, but naturally in practice there are many different shapes of load receptors and the location of the load will vary. Measurement Good Practice Guide No. To find out any hysteresis issues in the instrument, you need to calibrate with increasing and decreasing points. Often the calibration of weighing instruments is based on a quality system (such as ISO9000), health care, traffic (air, marine) safety or forensic investigation. endobj Weighing in the Pharmaceutical Industry T Scorer, M Perkin, M Buckley Measurement Good Practice Guide No. 5 0 obj<> on the weighing pan. Some weighing instruments are small laboratory instruments measuring a few grams and are very accurate. Many weighing instruments are used for legal measurements or measurements used as basis for monetary transfer and these are part of a legal or statutory verification program based on legislation. In case the weighing instrument fails in calibration and it is adjusted, you should make an “as found” calibration before adjustment and an “as left” calibration after adjustment. Standards OIML R76 and EN 45501 will give guidance for different load receptor shapes. That way it is easier to be sure that the load’s center of gravity is in the specified location. endstream Purpose: Purpose of this sop for operation, cleaning, verification, and calibration of bin lifting trolley with weighing balances.. As with any measurement instruments, weighing instruments should also be calibrated regularly to assure that they are measuring correctly and accurately. The test should preferably be done using just one test load, if possible. Chart 1. If the eccentricity test is used also to determine the errors of the indication, then a calibrated load should be used. c. When weighing, apply load to center of balance. The most common practice is the following: start with zeroing the instrument without any load. 3 0 obj<> Once the maximum load is recorded, start decreasing the loads through the decreasing test points. Drift check. Set the loads of the first test point, wait for stabilization, and record the indication. (error) within which a balance or scale is acceptable for mostsoillaboratory applications. Linearity issues means that the instrument does not measure equally accurate throughout the range. }=C�k�Y X��sHf�H{ea������:�x�AHь�S߸p�0�g�V���hPцI�e����3�#. 5.3 Switch ‘ON’ the balance. Likewise, with decreasing points, make sure that you approach each point with decreasing weight. endstream To find out the repeatability of the instrument, a repeatability test is done. Record the displayed weight in respective monthly calibration formats. 4 0 obj<> Picture below is a general illustration of hysteresis. In a weighing test, using multiple points through the measurement range of the instrument helps to reveal any issues with linearity. Repeat step 6 with the other weights. To download this article in as pdf file, please click the picture below: hbspt.cta._relativeUrls=true;hbspt.cta.load(2203666, '39ead636-70b8-4878-b308-90faa44f9c2b', {}); Let’s start by looking at some of the preparations you should make before the calibration and then look at the different tests you should be doing. 14 0 obj<>/ProcSet [/PDF /Text /ImageB /ImageC /ImageI]/Font<>>>/MediaBox[0 0 612 792]/Id(109)/StructParents 971/Rotate 0>> Scope: This sop is applicable to the trolley balance in the department at the plant.. RESPONSIBILITY: Officer production is responsible for verification. Heikki Laurila is Product Marketing Manager at Beamex Oy Ab. as needed. The functionality can be used either with a computer or with a mobile device. Typically, 5 to 10 different loads (test points) are used. You should find out the technical characteristics of the weighing instrument (max weight, d value), the accuracy requirement (max error allowed and uncertainty) and what to do if the calibration fails (adjustment). OIML R 111-1: 2004 (E) 5 2 TERMINOLOGY The terminology used in this Recommendation conforms to the International Vocabulary of Basic and General Terms in Metrology(1993 edition) [1] and the International Vocabulary of Terms in Legal Metrology(2000 edition) [2]. This means that when you increase the load, you must approach each test point with increasing weight. 16 0 obj <>stream Often the calibration of weighing instruments is based on a quality system (such as ISO9000), health care, traffic (air, marine) safety or forensic investigation. First, the load is placed in the center of the load receptor (the load’s center of gravity) and the result is observed. endobj endobj A proper metrologically traceable calibration is the only way to know how accurately weighing instruments are measuring. Alternatively, you may also tare the instrument when the load is in location number 1, as this makes it easier to see any difference between locations. Systematic evaluations of balance performance Great guidance on practices Even comparisons to test weighing emphasis on ≈20 mg M-5 mechanical balance w/ built –in weights 20 mg best precision 2 μg best 5 – 10 μg typical ≥20 μg can reach 100 μg NOW ?? 18, Version 4.0 (11/2015), EN 45501:2015 - Metrological aspects of non-automatic weighing instruments, NIST Handbook 44 (2017 Edition) - Specifications, Tolerances, and Other Technical Requirements for Weighing and Measuring Devices, U.S. Pharmacopeia Convention "Chapter 41 Balances" (2014)  (abbreviation "USP 41" used in blog text), EA-4/02 (2013) - Evaluation of the Uncertainty of Measurement in Calibration, JCGM 100:2008 - Evaluation of measurement data — Guide to the expression of uncertainty in measurement, JCGM 200:2008 - International vocabulary of metrology — Basic and general concepts and associated terms, OIML R76-1 - Non-automatic weighing instruments Part 1: Metrological and technical requirements - Tests, OIML R 111 - OIML R111: Weights of classes E1, E2, F1, F2, M1, M1-2, M2, M2-3 and M3, DIRECTIVE 2009/23/EC (2009) - Non-automatic weighing instruments. 1. Measurement uncertainty must be reported in a calibration certificate, otherwise it is invalid. x�+� � | balance has an on-board calibration function. 1 0 obj<> SOP No. More test points can be used for the typical range of usage of the instrument. Related: Drift and Its Importance in Analytical Balances 5.8 Daily Calibration of balance 5.8.1 Calibrate the balance daily with the standard weights of 1g, 10g, 100g, and 200g individually. The purpose of the minimum weight test is to find the smallest load that can be measured while still achieving reliable measurement results and fulfilling the accuracy requirements. 0�c�1T���sO��lS� endstream 8 0 obj <>stream What information should the calibration certificate include. hbspt.cta._relativeUrls=true;hbspt.cta.load(2203666, 'c12f2115-e1d4-498b-894d-337a48224e2e', {}); We exist to provide better ways to calibrate. Then the load is removed and zero indication is checked and zeroed if necessary. With multi-range instruments, each range is to be calibrated separately. You should not add too much weight and then remove it, because then you lose the hysteresis information. OIML Publications may be downloaded from the OIML web site in the form of PDF files. endobj VERIFYING CALIBRATION OF WEIGHING DEVICES USED FOR LABORATORY TESTING TXDOT DESIGNATION: TEX-901-K CONSTRUCTION DIVISION 3 – 5 EFFECTIVE DATE: AUGUST 1999 4.6 Procedure: 4.6.1 Clean the platform or pan, beams, display, etc. If any unevenness is observed in its location. endstream Finally, the test load is placed again to location 1 to check that the indication has not drifted from the earlier indication in location 1. The balance would come in the weighing mode. Make sure you have enough weights for the calibration procedure available. weighing scale. EQ-03-08 Date Revised 02-03-17 Page 5 of 6 . %���� CMX supports various tests such as: Eccentricity Test, Repeatability Test, Weighing Tests and Minimum Weighing Test. Aim: The SOP for calibration of weighing balance is applicable for all departments at plants. Let’s take a quick look of those: In addition to the above standard requirements, the requirements in the pharmaceutical industry requires a separate minimum weighing test, where a small test load is measured multiple times to find out the accuracy of the instrument with a small load. Additional information on OIML Publications may be obtained from the Organization’s headquarters: Bureau International de Métrologie Légale . Telephone: 33 (0)1 48 78 12 82 . 12 0 obj <>stream 8. 70 . endobj The calibration procedure should specify where to place the load during the test and calibration results (in certificate format) should also document the locations. Calibration Procedure for Analytical Balances and Scales. H��Wko�����a>ʀŐ"E�����l��Nj�XnQ�ȑ5�|-������;�a���#+3w���s�}��������W��g������/�>,߽_��Y���w���! Place the first Class 1 weight on the clean balance pan with plastic forceps, allow the balance to stabilize, measure and record the observed weight in the logbook. Balance calibration is the key service activity to ensure accurate weighing results. Has the principle that you calculate the measurement uncertainty for each calibration point and the smallest usable load is the point where the uncertainty is still small enough for the requirements for the instrument. Then the load is placed again, and so on. Apparatus 6.1 Precision Mass Srandards.-Precision mass stand-ards used for calibration ofbalances or scales must beof known accuracy. Often a repeatability test is done with one load only, but it can be done also with several different load values separately. 11 0 obj <>stream Strategies are presented to minimize errors associated with evaporation or other sample losses that might occur with the determination of mass by difference. He started working for Beamex in 1988 and has, during his years at Beamex, worked in production, the service department, the calibration laboratory, as quality manager, as product manager and as product marketing manager. number of decimal places over the whole operating range. 6 0 obj<> Test should be done in identical and constant conditions and with identical handling. endobj Uncertainty of calibration (estimates) Minimum weighing value Model Calibration point (No tare) Extended uncertainty (k=2) 0.001 mg BM-20 1 g 0.019 mg GH-202 50 g 0.17 mg Switch ON the balance. PDF | This paper describes the metrological requirements and the measurements methods for calibrating nonautomatic weighing instruments. x�u��N�0�w?�[ �QKԭ�T1C�:����U���IX�]���9�ʼn|�z���H���rp��+Ob�7=Y�6��Vuh���F��|�b-o�|��0{m�+}^OR��;��uR�D��*�J��L����%�ž�0DM����*�`���7O�c���1���\��,趠�����XHޡV G�� The indication is zeroed before the test. In some cases, the weighing instrument may be calibrated with increasing loads only or decreasing loads only. endobj 11, rue Turgot - 75009 Paris - France . 2 0 obj<> hbspt.cta._relativeUrls=true;hbspt.cta.load(2203666, '442f8420-1250-4492-a8c1-495c64a5b587', {}); hbspt.cta._relativeUrls=true;hbspt.cta.load(2203666, '2bb3f24d-7be7-4c00-b526-028ac6ed7bd9', {}); The most relevant references for this subject include, but not limited to, following: Topics: EURAMET Calibration Guide No. Internet: www.oiml.org . Before you can start the calibration of the weighing instrument, you should clarify a few things and get prepared. We all see weighing instruments in our everyday life around us, for instance, when we visit a grocery store and weigh vegetables. What kind of things will cause uncertainty in the calibration of weighing instruments? Next, the load is placed in four different sectors of the load receptor, as illustrated in the picture below. balances used for calibration of pipettes, and for their two parameters: repeatability and linearity. Date Calibration Reading Initials Date Calibration Reading Initials Date Calibration Reading Initials BALANCE CALIBRATION LOG PHARMACY NAME: Check out our other product lines:, After the … endobj The weighing instrument should not be used to measure any loads smaller than the minimum load. Blacklead Island Sunday, November 10, 2019 3:06:42 PM. On laboratory balances, be sure that no debris or portion of a plastic cover restricts pan movement. 3. 12.3 Six Month Accuracy Check of Weigh Balances a. Certified calibration weight supplied as standard Can be connected to RS232 interface Labocon Analytical Balance LAB-100 Series can be used in Laboratories, Pharmaceuticals and Research . weighing instrument, The smallest test load can be 10% of the maximum load, or the smallest weight normally used. 4 . The zero may be checked between each location to see that it has not changed. The highest load should be close to the maximum of the instrument. Posted January 16, 2020 by Kevin Hill & filed under analytical balances.. Even the zero and full span are correct, there may be errors in the middle of the range, which is referred as linearity errors, or unlinearity (or nonlinearity). As the aim of the eccentricity test is to find out the difference caused by the location of the load, it is not necessary to have an accurate calibrated load. Himself, his wife and their four children OIML web site in the form PDF. 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